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Manufacturing of Photoactive β-Bismuth Oxide by Flame Spray Oxidation

dc.contributor.authorFerrer, Martha
dc.contributor.authorMuñoz-Saldaña, J.
dc.contributor.authorAyala-Ayala, M. T.
dc.date.accessioned2021-12-10T21:08:22Z
dc.date.available2021-12-10T21:08:22Z
dc.date.issued2021-03-21
dc.identifier.urihttp://repositorio.ufps.edu.co/handle/ufps/5924
dc.description.abstractPhotoactive tetragonal bismuth oxide powder with different semiconducting characteristics was synthesized from Bi-pellets by flame spray oxidation. The effect of feedstock particle size and standoff distance (SOD) on the physical properties of β-Bi2O3 keeping constant the fuel/oxygen ratio is here reported. The flame spray oxidized powder was collected either from evaporated or in-flight particles quenched in water. The combination of flame spray processing parameters led to different β-Bi2O3 phase contents, oxidation characteristics, size distribution (nanometric and micrometric sized), morphology, and optical properties of the sprayed powder. The highest micrometric β-Bi2O3 content quenched in water was obtained at a SOD of 30 cm using a particle size distribution of 12-60 μm of Bi-feedstock. The obtained powder from in-flight particles collected in water allowed us to analyze the oxidation characteristics of bismuth. Micrometric powder shows the synthesis of snowman-like Bi/β-Bi2O3 Janus particles. The nanometric sized Bi2O3 powder was continuously obtained by spray oxidation, where its collection efficiency depends on processing parameters and showed spherical morphology and a highly pure tetragonal phase with narrow visible light absorbance (Eg = 2.26 eV). These optical characteristics indicate that the obtained β-Bi2O3 powder is suitable for high-performance visible-light photocatalyst.eng
dc.format.mimetypeapplication/pdfspa
dc.language.isoengspa
dc.publisherJournal of Thermal Spray Technologyspa
dc.relation.ispartofJournal of Thermal Spray Technology
dc.rightsSpringer Nature has partnered with Copyright Clearance Center's RightsLink service to offer a variety of options for reusing this content.eng
dc.sourcehttps://link.springer.com/article/10.1007%2Fs11666-021-01182-2spa
dc.titleManufacturing of Photoactive β-Bismuth Oxide by Flame Spray Oxidationeng
dc.typeArtículo de revistaspa
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dc.identifier.doi10.1007/s11666-021-01182-2
dc.relation.citationeditionVol.30 (2021)spa
dc.relation.citationendpage1119spa
dc.relation.citationstartpage1107spa
dc.relation.citationvolume30spa
dc.relation.citesAyala-Ayala, M.T., Ferrer-Pacheco, M.Y. & Muñoz-Saldaña, J. Manufacturing of Photoactive β-Bismuth Oxide by Flame Spray Oxidation. J Therm Spray Tech 30, 1107–1119 (2021). https://doi.org/10.1007/s11666-021-01182-2
dc.relation.ispartofjournalJournal of Thermal Spray Technologyspa
dc.rights.accessrightsinfo:eu-repo/semantics/restrictedAccessspa
dc.subject.proposalflame spray oxidationeng
dc.subject.proposaloptical propertieseng
dc.subject.proposaltetragonal bismuth oxideeng
dc.subject.proposalvisible-light photocatalysteng
dc.type.coarhttp://purl.org/coar/resource_type/c_6501spa
dc.type.contentTextspa
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oaire.versionhttp://purl.org/coar/version/c_970fb48d4fbd8a85spa
dc.type.versioninfo:eu-repo/semantics/publishedVersionspa


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