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dc.contributor.authorOlaya, Jhon
dc.contributor.authorBautista-Ruiz, Jorge
dc.contributor.authorAlfarez, Fabio Leonardo
dc.date.accessioned2021-12-08T19:41:55Z
dc.date.available2021-12-08T19:41:55Z
dc.date.issued2018-10
dc.identifier.urihttp://repositorio.ufps.edu.co/handle/ufps/1748
dc.description.abstractEn este trabajo se presenta la síntesis y la evaluación de la resistencia a la corrosión de recubrimientos de SiO2-TiO2-ZrO2-BiO2 depositados por la técnica de centrifugado sobre acero inoxidable AISI 316L. Los soles se prepararon a partir de una mezcla de precursores orgánicos, como el tetraetoxisilano (TEOS) al 98%, tetrabutóxido de titanio (TBT) al 97%, zirconio (IV) butóxido (TBZ) al 80% en solución 1-butanol y nitrato de bismuto penta-hidratado Bi(NO3)3*5H2O. La resistencia a la corrosión se determinó mediante ensayos de curvas de polarización potenciodinámica y de espectroscopia de impedancia electroquímica (EIS) en una solución electrolítica de 3,5% Wt de NaCl + 0,5 M de H2SO4. A los soles preparados se les caracterizó mediante estudio reológico, de pH en función del tiempo, mediciones de espectroscopia de infrarrojo por transformada de Fourier (FTIR) y calorimetría diferencial de barrido (DSC). Los recubrimientos se caracterizaron mediante difracción de rayos X (XRD), microscopia electrónica de barrido (MEB), espectroscopia de energías dispersivas (EDX), fluorescencia de rayos X (XRF) y medidas de adherencia. Los resultados mostraron que las películas ofrecen una buena resistencia a la corrosión sobre el sustrato metálico disminuyendo los valores de densidades de corriente hasta en un orden de magnitudspa
dc.description.abstractThis report show the synthesis and corrosion resistance of SiO2-TiO2-ZrO2-BiO2 coatings deposited by spin-coating on AISI 316L stainless steel. The soles were prepared from a mixture of organic precursors, such as 98% tetraethoxysilane (TEOS), titanium tetrabutoxide (TBT) 97%, Zirconium (IV) butoxide (TBZ) 80% in 1-butanol solution and bismuth penta nitrate-hydrate Bi (NO3)3*5H2O. The coatings were evaluated by potentiodynamic polarization and Electrochemical Impedance Spectroscopy (EIS) test in an electrolytic solution of 3.5% Wt NaCl + 0.5 M H2SO4. The soles prepared were studied trough rheological, pH as a time function, Fourier Transform Infrared Spectroscopy (FTIR) and differential scanning calorimetry (DSC) analysis. The coating were characterized by X ray diffraction (XRD), scanning electron microscopy (SEM) and dispersive energy spectroscopy (EDX), X ray fluorescence (XRF) and adhesion measurements. The results showed that the films offer good corrosion resistance on the metal substrate, decreasing current densities up to one order of magnitude.eng
dc.format.mimetypeapplication/pdfspa
dc.language.isospaspa
dc.publisherBoletin de la Sociedad Espanola de Ceramica y Vidriospa
dc.relation.ispartofBoletin de la Sociedad Espanola de Ceramica y Vidrio
dc.rights0366-3175/© 2018 SECV. Publicado por Elsevier Espana, ˜ S.L.U. Este es un art´ıculo Open Access bajo la licencia CC BY-NC-ND (http:// creativecommons.org/licenses/by-nc-nd/4.0/).spa
dc.sourcehttps://www.sciencedirect.com/science/article/pii/S0366317518300141spa
dc.titleSynthesis and corrosion resistance evaluation of coatings of SiO2-TiO2-ZrO2-BiO2 on 316L stainless produced by sol-geleng
dc.typeArtículo de revistaspa
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dc.identifier.doihttps://doi.org/10.1016/j.bsecv.2018.02.001
dc.publisher.placeMadrid , Españaspa
dc.relation.citationeditionVol.57 No.5.(2018)spa
dc.relation.citationendpage206spa
dc.relation.citationissue5 (2018)spa
dc.relation.citationstartpage195spa
dc.relation.citationvolume57spa
dc.relation.citesLeonardo Alferez, F., Jairo Olaya, J., & Hernando Bautista, J. (2018). Synthesis and corrosion resistance evaluation of coatings of SiO2-TiO2-ZrO2-BiO2 on 316L stainless produced by sol-gel. BOLETIN DE LA SOCIEDAD ESPANOLA DE CERAMICA Y VIDRIO, 57(5), 195-206.
dc.relation.ispartofjournalBoletin de la Sociedad Espanola de Ceramica y Vidriospa
dc.rights.accessrightsinfo:eu-repo/semantics/openAccessspa
dc.rights.creativecommonsAtribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)spa
dc.subject.proposalSol-gelspa
dc.subject.proposal316Lspa
dc.subject.proposalRecubrimientospa
dc.subject.proposalCompuesto de (SiO2-TiO2-ZrO2-BiO2)spa
dc.subject.proposalCorrosiónspa
dc.subject.proposalAdherenciaspa
dc.subject.proposalCoatingeng
dc.subject.proposal(SiO2-TiO2-ZrO2-BiO2) compositeeng
dc.subject.proposalCorrosioneng
dc.subject.proposalAdherenceeng
dc.title.translatedSynthesis and corrosion resistance evaluation of coatings of SiO2-TiO2-ZrO2-BiO2 on 316L stainless produced by sol-gel
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