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    • Effect of nitrogen flow ratio on microstructure, mechanical and tribological properties of TiWSiN x thin film deposited by magnetron co-sputtering 

      Olaya, Jhon; Macias Ramirez, Hugo Alejandro; Aperador Chaparro, William Arnulfo; Yate, L; L.E, Coy (Applied Surface ScienceBogota , Colombia, 2018-10-31)
      We investigate the deposition of TiWSiNx thin films by means of the method of reactive magnetron co-sputtering, setting the nitrogen flow ratios N2/(Ar + N2) at 4.8%, 9.1%,16.7 and 33.3%. The crystallographic structure of ...
    • Experimental characterization of the mechanical properties of PETG and PA6 thermoplastics 

      Coba Salcedo, Milton Fabian; Acevedo Peñaloza, Carlos Humberto; Guerrero Gomez, Gustavo (Contemporary Engineering SciencesBulgaria, 2018-09-12)
      Simple thermoplastic materials and polymer matrix composites have been used in this work. Polyethylene terephthalate glycol (PETG) plates, a copolymer of CHDM- cyclohexane dimethanol modified polyethylene terephthalate ...

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      • Portada Effect of nitrogen flow ratio on microstructure, mechanical and tribological properties of TiWSiN x thin film deposited by magnetron co-sputtering

        Effect of nitrogen flow ratio on microstructure, mechanical and tribological properties of TiWSiN x thin film deposited by magnetron co-sputtering

        ...

        Olaya, Jhon | 2018-10-31

        We investigate the deposition of TiWSiNx thin films by means of the method of reactive magnetron co-sputtering, setting the nitrogen flow ratios N2/(Ar + N2) at 4.8%, 9.1%,16.7 and 33.3%. The crystallographic structure of the films was established through X-ray diffraction (XRD), the morphology and topography were evaluated through scanning electron microscopy (SEM) and atomic force microscopy (AFM), the chemical composition was evaluated through X-ray diffraction and X-ray photoelectron spectroscopy, the mechanical properties were evaluated by nanoindentation, and the wear resistance was studied via nanowear and pin-on-disk. It was found that films deposited between 4.8% and 16.7% nitrogen flow ratio exhibited an amorphous phase. As the nitrogen was increased, the films evolved into a mixture of amorphous Si3N4 and crystalline TiWN phase. Moreover, the film morphology changed to fine columnar as the nitrogen flow ratio increased. As a general observation, the hardness, resistance to plastic deformation (H3/E2), and residual stress of the samples increased as the nitrogen flow ratio increased. The maximum hardness, resistance to plastic deformation, and residual stress were 22 ± 0.4 GPa, 213 ± 20 MPa, and 1.4 ± 0.01, respectively. The lowest nanowear volume (0.47 µm3) and wear rate (11 ± 8 10−9 mm3/N mm) were obtained for films deposited at high nitrogen flow ratios. The lowest friction coefficient (0.15) was recorded for films deposited at 16.7% nitrogen flow ratio.

        LEER

      • Portada Experimental characterization of the mechanical properties of PETG and PA6 thermoplastics

        Experimental characterization of the mechanical properties of PETG and PA6 thermoplastics

        ...

        Coba Salcedo, Milton Fabian | 2018-09-12

        Simple thermoplastic materials and polymer matrix composites have been used in this work. Polyethylene terephthalate glycol (PETG) plates, a copolymer of CHDM- cyclohexane dimethanol modified polyethylene terephthalate [56], were used, which is an amorphous and therefore transparent material, which was available in plates or extruded sheets in a wide range of thicknesses. The PETG sheets are of commercial type and their production process is carried out by the company that supplied them. Also part of the study is polyamide 6.6 with 30% short glass fibre content obtained by injection moulding and compression moulding, which was supplied by the ESIS TC4, for the first Round Robin of short glass fibre composite materials.

        LEER

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