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    • Optimization of the Tensile Properties of Polymeric Matrix Composites Reinforced with Magnetite Particles by Experimental Design 

      LARA GONZÁLEZ, LUIS ÁNGEL; RODRÍGUEZ LÓPEZ, WILMAR GUILLERMO; Pineda Triana, Yaneth; Peña Rodriguez, Gabriel; Felipe, Hugo (TecnoLógicasBogota , Colombia, 2020-05-15)
      A full-factorial 33 experiment was used in this study to determine the optimal values of the tensile properties of three composite materials manufactured based on three polymeric resins: Derakane Momentum epoxy vinyl ester ...
    • Production and structural, electrical and magnetic characterization of a composite material based on powdered magnetite and high density polyethylene 

      Garzón, Andrés; Landínez, David A.; Roa-Rojas, Jairo; Fajardo Tolosa, Fabio Enrique; Peña Rodriguez, Gabriel; Parra-Vargas, C.A (Revista De La Academia Colombiana De Ciencias Exactas, Físicas Y NaturalesColombia, 2017-06-30)
      This work describes the production and characterization of a composite material based on magnetite filled HDPE, which is commonly known for its magnetic properties. Composites of this kind are used in different ...

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      • Portada Optimization of the Tensile Properties of Polymeric Matrix Composites Reinforced with Magnetite Particles by Experimental Design

        Optimization of the Tensile Properties of Polymeric Matrix Composites Reinforced with Magnetite Particles by Experimental Design

        ...

        LARA GONZÁLEZ, LUIS ÁNGEL | 2020-05-15

        A full-factorial 33 experiment was used in this study to determine the optimal values of the tensile properties of three composite materials manufactured based on three polymeric resins: Derakane Momentum epoxy vinyl ester based on bisphenol-A (DM-411), polyester based on terephthalic acid (P115-A), and isophthalic polyester (P2000). Such materials were reinforced with magnetite powders at concentrations of 10, 20, and 30 wt %, and the particle sizes were classified with three sieves: #200 (46–75 μm), #325 (26–45 μm), and #500 (0–25 μm). The compounds were manufactured using the hand lay-up method at room temperature in accordance with ASTM D638-14 for M1-type specimens. A tensile test was conducted on a universal Microtest EM2/300/FR machine at a test speed of 5 ± 25 % mm/min using an Epsilon extensometer calibrated in accordance with the ASTM E83 standard at 20 ± 2 °C. The magnetite powders and compound morphology were studied by Scanning Electron Microscopy. The mechanical properties of the compounds and the optimal response found by Analysis of Variance (ANOVA) and Response Surface Methodology (RSM) are also reported. The best response to the mechanical stimuli occurs with the composite material prepared with the epoxy vinyl ester resin DM-411, a concentration of 29.4 % of magnetite (Fe3O4), a particle size of 58.5 microns, and a 200 sieve.

        LEER

      • Portada Production and structural, electrical and magnetic characterization of a composite material based on powdered magnetite and high density polyethylene

        Production and structural, electrical and magnetic characterization of a composite material based on powdered magnetite and high density polyethylene

        ...

        Garzón, Andrés | 2017-06-30

        This work describes the production and characterization of a composite material based on magnetite filled HDPE, which is commonly known for its magnetic properties. Composites of this kind are used in different applications such as microwave absorption, transducers and biomedical applications like drug delivery, organs tagging, etc. The samples were produced according to different volume ratios of magnetite and HDPE. The semiquantitative analysis conducted by XRD revealed the presence of hematite within the mineral magnetite used as a filler in the composites. The crystallinity degree was calculated through X-ray diffraction tests. The XRD results showed how there is an amorphous-crystalline transition due to the magnetite increasing content. The crystallinity percent (χc ) for samples filled with 40% of magnetite volume was 90% while the (χc ) for samples filled with 10% of magnetite volume was 80%. Which may be related to the increased magnetite particles into the plastic matrix for reinforcement contents up to 30% by volume, as evidenced in the images obtained through scanning electron microscopy (SEM). The samples were electrically characterized through volume resistivity measurements and electric polarization. The results showed that for ratios less than the 20% of magnetite there is no substantial reduction in the resistivity of the composite samples compared to the unfilled HDPE samples, but for magnetite ratios above 30% the composite samples showed a substantial reduction of six orders of magnitude in their volumetric resistivity. The electric polarization showed how the composite material undergoes a transition, going from an insulating material (for samples with 10% of magnetite volume) to a resistive material where the current and voltage are in phase (for samples with 30% and 40% of magnetite volume). The magnetization curves showed that the saturation magnetization (from 17,3 to 60,5 emu/g) and remanence (from 0,94 to 5 emu/g) increase in samples with high magnetite contents. The presence of the hematite phase in the samples could have affected the magnetization saturation and the remanence values in the hysteresis curves. Magnetization curves as a function of temperature showed the Verwey samples transition around the 120K and confirmed that the magnetization increases as the magnetite volume within the matrix increases. © 2017. Acad. Colomb. Cienc. Ex. Fis. Nat.

        LEER

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